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1 4 which was converted to 3a by reduction and saponification.
2 g carboxyl moieties, which can be removed by saponification.
3 available tri-O-acetyl-d-glucal followed by saponification.
4 d derivative 19 with diethyl L-glutamate and saponification.
5 sulating thermoplastic (polylactic acid) via saponification.
6 coupled with diethyl l-glutamate followed by saponification.
7 coupled with diethyl L-glutamate followed by saponification.
8 coupled with diethyl-l-glutamate followed by saponification.
9 up compatibility of beta-hydroxy phosphonate saponification.
10 resistance of the product of the reaction to saponification.
11 ma was analyzed in a similar way but without saponification.
12 target analogues 10 were readily prepared by saponification.
13 ied base concentration and the total time of saponification across a wide range and again used HPLC t
20 ction and the total sterolic fraction, after saponification and acidic hydrolysis of the samples, are
24 results of four soybeans using the described saponification and HPLC analytical method was validated
30 as vitamin A palmitate) without the need for saponification and validated it in model systems consist
31 alkylation with methyl bromoacetate in DMF, saponification, and cyclization with acetic anhydride an
32 hlorophyll removal mechanism is not based on saponification, apolar adsorption or anion exchange, but
33 -6-(bromomethyl)-pteridine followed by ester saponification at room temperature to afford the respect
35 ves the corresponding amino ester that, upon saponification, can be protected with the fluorenylmethy
36 with trimethylsulfoxonium ylide, followed by saponification, completed a five-step synthesis of 1 in
37 tion of the beta-indole-alpha-oximinoesters, saponification, condensation with symmetrical diamines,
39 arachidonoyl)-phosphatidylethanolamine under saponification conditions, and the amount produced incre
42 standards were added as surrogates prior to saponification, correcting for extraction inefficiencies
44 pimerization of the ester center followed by saponification/crystallization affords the desired hydro
46 erial from the Eskimo mummy was subjected to saponification, extraction, and digitonin precipitation.
51 terol was isolated from whole yeast cells by saponification, followed by extraction of nonsaponifiabl
54 diluted in hexane without derivatisation or saponification, greatly reducing sample preparation time
55 ommon entities that can occur are pancreatic saponification, heterotopic mesenteric ossification, and
56 scalemic diesters 4 with t-BuLi, followed by saponification in the presence of air, gave 2,2'-di-tert
57 y acidity, peroxide, iodine, refractive, and saponification indexes, beyond moisture, lipid and free
58 rted in five steps (reduction of the ketone, saponification, iodolactonization, ozonolysis, and intra
61 o avoid carotenoid artifact formation during saponification, Larsen and Christensen (2005) developed
62 t-saving method, based on microwave-assisted saponification (MAS) followed by epoxidation and on-line
67 l and chemical parameters (melting point and saponification number), and the fraction of hydrocarbons
71 rganic base KHCO(3) was employed to minimize saponification of a particularly sensitive lactone subst
73 ine F, and fragments 88 and 89 obtained upon saponification of batzelladine F, demonstrated that the
75 ters are accessible by the selective partial saponification of dimethyl or diethyl alkyl phosphonates
76 Yamaguchi macrolactonization, and selective saponification of ester moiety in the presence of a lact
81 e percentage of KOH (60% and 80% w/v) in the saponification of samples for the determination of alpha
84 eria in an extraction vessel resulted in the saponification of the bacterial lipids and derivatizatio
85 ing opening with cesium benzoate followed by saponification of the benzoate to afford (+)-pancratista
87 anopyrrolo[2,3-d]pyrimidine (28) followed by saponification of the ethyl esters, for the classical an
92 the primary alcohol group in 50 followed by saponification of the two remaining ester groups gave 3.
95 ce acid and base injury, cell death, and the saponification of triglycerides in ex vivo porcine adipo
96 the cyclopentenones (e.g., demethylation and saponification) of the CNTs lead to demethylated or hydr
97 e solubilized by proteolytic digestion after saponification, of which involucrin was the most abundan
99 quisite triesters were prepared by selective saponification or by the prior incorporation of one benz
100 also proposed to avoid tedious steps such as saponification or derivatization before gas chromatograp
101 acid and amine derivatives were obtained by saponification or HCl acidolysis of o-boronato-phosphoni
103 rational parameters were optimized for a hot saponification procedure and utilizing fractional precip
105 aces analysis showed that the most efficient saponification procedure was obtained using a 60% (w/v)
106 tina, and to assess the effects of different saponification procedures on the recovery of quail retin
108 ich is then followed by a uniquely effective saponification reaction of 23c using anhydrous hydroxide
109 dy identified that soap, produced during the saponification reaction, resulted in a significant reduc
110 The simplified one-step extraction without saponification significantly increased the recovery of t
111 total time of extraction for 300s regarding saponification step when compared to 3600s from the trad
112 ng a time-consuming and possibly detrimental saponification step, followed by extraction and HPLC ana
113 ally, it was proposed for the removal of the saponification step, which simplifies the extraction pro
115 ; however, these polymers are susceptible to saponification that can result from harsh preparation or
117 rent preparative parameters, such as time of saponification, the type of organic solvents for fat ext
119 ical dipyrrylmethane 19, and following ester saponification, this was condensed with a dipyrrylmethan
120 of simultaneously extracting sterols during saponification thus significantly reducing extraction ti
122 goes a kinetically controlled epimerization/ saponification to afford the pure trans-pyrrolidine carb
123 l ester of ciprofloxacin (11) to give, after saponification to remove all of the esters, the desired
124 iabetic rats, before and after conversion by saponification to the corresponding DKP insulin enantiom
125 reated human foreskin CEs with methanol/KOH (saponification) to hydrolyze off much of the lipids.
128 g of oil), acid value (2.36mg KOH/g of oil), saponification value (183.8mg KOH/g of oil), peroxide va
130 ere as follows: melting point, 45 degrees C; saponification value, 202.3 mg KOH/g oil; refractive ind
135 solvent ratio of 1:10 (w/v) was optimal, and saponification was performed at 80 degrees C for 1 h.
136 atty acids extracted from cell pellets after saponification were analyzed by gas chromatography/mass
140 ts were dissolved in chloroform with help of saponification with 1M solution of sodium hydroxide in u
141 mg/100 g DW) was able to be extracted after saponification with acidified phosphate buffer, instead