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3 5% dichloroacetic acid (DCA) and successive heteronuclear (1)H-(15)N HSQC spectra were collected to
4 H-(1)H nuclear Overhauser effects (NOEs) and heteronuclear (1)H-(15)N NOEs if the paramagnetic contri
7 lycan binding, we performed multidimensional heteronuclear ((1)H, (13)C, (15)N) NMR (nuclear magnetic
8 t LPS was analyzed by homonuclear ((1)H) and heteronuclear ((1)H,(13)C, and (1)H,(31)P) correlated on
10 ift values as well as both one- and two-bond heteronuclear (13)C-(77)Se coupling constants, and the c
11 two-dimensional ((1)H-(1)H) homonuclear and heteronuclear ((13)C-(1)H) single quantum correlations (
12 that combines measurements of R1, R1rho, and heteronuclear 13C{1H} NOEs for protonated base (C2, C5,
14 relaxation data ((15)N-T(1), (15)N-T(2), and heteronuclear (15)N-{(1)H}-nOe) recorded on all three ap
16 Fluorine observed homonuclear 19F-19F and heteronuclear 19F-1H NOE experiments providing selective
18 so evident in the F2 hydrogen dimension from heteronuclear 1H-13C HSQC spectroscopy, which did not de
19 hydrophobic core of a protein, demonstrating heteronuclear 1H-15N NMR data on the Lys-66 side chain a
20 LC, and combined analysis of homonuclear and heteronuclear (2,3)J couplings, along with ROE data.
23 ive nuclei of the ChB-donor chalcogen atoms, heteronuclear (77)Se and (125)Te NMR were used to direct
24 nt of the integrated intensity obtained in a heteronuclear and a homonuclear spin-echo experiment, S(
25 ling scheme, termed sel-SHARPER, removes all heteronuclear and homonuclear couplings of the selected
26 asis for the formation of both the homo- and heteronuclear bimetallics, for the observed two-electron
27 ted, such as in the acquisition dimension of heteronuclear broadband decoupled HSQC (heteronuclear si
29 ermined by experiments that probe long-range heteronuclear contacts for fibrils templated from a 1:1
33 solid-state two-dimensional (2D) (13)C{(1)H} heteronuclear correlation (HETCOR) NMR analyses support
34 resolved in the two-dimensional (2-D) 1H-17O heteronuclear correlation (HETCOR) NMR spectra allowing
35 al-echo double resonance (CP-REDOR) NMR, and heteronuclear correlation (HETCOR) NMR spectroscopy to d
36 2D) (13)C-(1)H, (13)C-(19)F and (19)F-(29)Si heteronuclear correlation (HETCOR) spectra were obtained
37 h-resolution two-dimensional (2D) (1)H-(15)N heteronuclear correlation (HETCOR) spectroscopy has been
38 1)H-based SSNMR study [1D (1)H and 2D (1)H-X heteronuclear correlation (HETCOR, X = (13)C, (29)Si) ex
39 ple set, the quality of a protein's [15N-1H]-heteronuclear correlation (HSQC) spectrum recorded under
40 D (29)Si{(1)H}, (13)C{(1)H}, and (31)P{(1)H} heteronuclear correlation and 1D (29)Si{(13)C} rotationa
42 ydroxide ion was found, through a (1)H-(31)P heteronuclear correlation experiment, to be confined to
43 lica has been established by two-dimensional heteronuclear correlation experiments involving 1H, 11B,
46 CH(n) selection, two-dimensional (1)H-(13)C heteronuclear correlation NMR (2D HETCOR), 2D HETCOR com
52 present new sensitivity enhanced schemes for heteronuclear correlation spectroscopy (HETCOR) in solid
55 ss-polarization, (13)C{(1)H} two-dimensional heteronuclear correlation, and (1)H relaxation technique
56 MBC) optimized to detect four- and five-bond heteronuclear correlations and the use of computer-assis
57 the spectral coordinates observed in the 2D heteronuclear correlations, previously postulated interm
58 s determined from a combination of homo- and heteronuclear coupling constants in conjunction with mol
59 mplished by consideration of homonuclear and heteronuclear coupling constants in tandem with ROESY da
60 ional NMR approaches based on both homo- and heteronuclear couplings ((1)H-(1)H COSY; (1)H-(13)C HSQC
61 , we introduce the application of scaling of heteronuclear couplings by optimal tracking (SHOT) to ac
62 single selected signal, SHARPER removes all heteronuclear couplings of a selected nucleus without th
63 pectra in natural abundance samples based on heteronuclear couplings to these same, (13)C-bonded nucl
66 ediate-sized molecules, however, show strong heteronuclear cross-relaxation effects: spontaneous proc
67 r the accurate measurement of intermolecular heteronuclear cross-relaxation rates by simultaneous acq
68 n a broader context, accurate measurement of heteronuclear cross-relaxation rates may enable the stud
70 e applied here combines both homonuclear and heteronuclear details and therefore provides complete in
71 yielded site-specific (1)H-(13)C/(1)H-(15)N heteronuclear dipolar coupling constants for CAP-Gly and
72 sociated (15)N chemical shift and (1)H-(15)N heteronuclear dipolar coupling frequencies as orientatio
73 SLF techniques to accurately measure strong heteronuclear dipolar couplings between directly bonded
75 used for the measurement of a broad range of heteronuclear dipolar couplings, allowing for a complete
76 t suitable for the measurement of long-range heteronuclear dipolar couplings, and that they provide i
77 conformational order parameters are based on heteronuclear dipolar couplings, and they are correlated
78 xation of the hyperpolarized LLS, induced by heteronuclear dipolar couplings, generates strongly enha
81 resent an approach for (1)H-(13)C/(1)H-(15)N heteronuclear dipolar recoupling under fast MAS conditio
82 age the static chemical shift anisotropy and heteronuclear dipole-dipole coupling powder patterns to
87 hievement of two-dimensional (2D) (1)H-(13)C heteronuclear experiments with a precision of a few per
90 the reactants are aligned and activated by a heteronuclear four-metal-ion center that contains a meta
91 lude a homonuclear all-Ru hexamer as well as heteronuclear hexamer and nonamer with alternating Ru/Ru
92 d to selected peaks from the two-dimensional heteronuclear HSQC spectrum of a sample of natural organ
94 1, and that IL-1beta and IL-1alpha stimulate heteronuclear I-1beta splicing and translation of the ne
96 e 15N transverse coherence (termed HISQC for heteronuclear in-phase single quantum coherence spectros
103 ipolar dephasing followed by proton-assisted heteronuclear magnetization transfer yields long-range (
104 ransmetalation agents for the preparation of heteronuclear molecular gold carbido complexes such as [
105 owing to multiphoton absorption, which in a heteronuclear molecular system occurs predominantly loca
113 eronuclear Multiple Quantum Coherence and 2D Heteronuclear Multiple Bond Coherence spectroscopic anal
114 eteronuclear sequential quantum correlation, heteronuclear multiple bond correlation) analysis identi
115 ties for NH3 cross-peaks than either HSQC or heteronuclear multiple quantum coherence (HMQC) correlat
116 e site loop is suppressed and the (1)H-(13)C heteronuclear multiple quantum coherence (HMQC) spectrum
119 r single quantum correlation) and fast-HMQC (heteronuclear multiple quantum correlation) pulse sequen
122 pectroscopy, total correlation spectroscopy, heteronuclear multiple-quantum coherence, and NOE, were
124 effects (fluoro, nitrobenzoate), handles for heteronuclear NMR ((19)F:fluoro; pentafluorophenyl or pe
131 or enzymatic oxidation in rat liver cytosol; heteronuclear NMR experiments revealed that oxidation oc
132 ing one- and two-dimensional (1)H, (13)C and heteronuclear NMR experiments under continuous flow.
134 achieved by two-dimensional homonuclear and heteronuclear NMR experiments, is reported for the first
135 near-UV CD, fluorescence, urea titration and heteronuclear NMR experiments, we show that three amino
136 reliable way of enhancing the sensitivity of heteronuclear NMR in dilute mixtures of metabolites.
140 15N-labeled PSA, we applied a combination of heteronuclear NMR methods, such as heteronuclear single
142 nt helix at low temperature as identified by heteronuclear NMR relaxation measurements, secondary che
144 ntent, leading to remarkably clean homo- and heteronuclear NMR spectra of the serum metabolome that c
146 flexibility in the native state as probed by heteronuclear NMR spectroscopy and multiple conformer si
147 red the autocatalytic conversion of BACE1 by heteronuclear NMR spectroscopy and used chemical shift p
150 of the two sequences using multidimensional heteronuclear NMR spectroscopy, and the structure was fo
157 h as may be obtained from a two-dimensional, heteronuclear NMR spectrum), the inverse mode of SPARIA
162 er acidic conditions, using a combination of heteronuclear NMR, analytical ultracentrifugation, and c
163 Using UV melting, gel electrophoresis and heteronuclear NMR, we investigated effects of various si
169 e serine were analyzed using R(1), R(2), and heteronuclear NOE experiments, variable temperature TROS
175 tion rates ( (15)N R 1, R 2) and (1)H- (15)N heteronuclear NOE values indicated that HscB is rigid al
176 lyses, d(NN)(i, i + 1) NOEs, and (15)N{(1)H} heteronuclear NOE values show that the C-terminal subdom
177 These regions also have small but positive heteronuclear NOEs, interresidue d(NN) NOEs, and small b
178 ) and T(2) relaxation times and {(1)H}-(15)N heteronuclear NOEs, reveal residue flexibility at the ac
179 dom-coil values, and by measuring (1)H-(15)N heteronuclear NOEs, which are all consistent with an unf
180 e frameshift site RNA using multidimensional heteronuclear nuclear magnetic resonance (NMR) methods.
182 tween PIDD-DD and RAIDD-DD in solution using heteronuclear nuclear magnetic resonance (NMR) spectrosc
185 e (R1), transverse relaxation rate (R2), and heteronuclear nuclear Overhauser effect (NOE)] measured
189 ied beta-strand was confirmed by T1, T2, and heteronuclear nuclear Overhauser enhancement (NOE) measu
190 Using high-resolution NMR experiments of heteronuclear nuclear Overhauser enhancement (NOE), spin
191 , is introduced that allows the detection of heteronuclear one-bond correlations in less than 30 s on
192 and transverse relaxation rates and [1H]-15N heteronuclear Overhauser effects of the backbone amides
194 iffusion-ordered NMR spectroscopy as well as heteronuclear Overhauser enhancement NMR spectroscopy.
195 substances was verified by either (19)F-(1)H heteronuclear Overhauser spectroscopy (HOESY) or X-ray c
202 ntrast, acute stress increased levels of PPG heteronuclear RNA (hnRNA) in a glucocorticoid-dependent
203 ing that SAA increased expression of sPLA(2) heteronuclear RNA and that inhibiting transcription elim
206 PSF3), an essential component for converting heteronuclear RNA to mRNA, binds with high affinity to t
210 gh-resolution-MS and NMR ((1)H, (13)C, COSY, heteronuclear sequential quantum correlation, heteronucl
211 construction, and J-compensated quantitative heteronuclear single quantum (HSQC) (1)H-(13)C NMR spect
212 INEPT), correlation spectroscopy (COSY), and heteronuclear single quantum coherence (HSQC) are also d
213 ches have been proposed utilizing (1)H-(15)N heteronuclear single quantum coherence (HSQC) as well as
214 apes of NH3 signals in a conventional 1H-15N heteronuclear single quantum coherence (HSQC) correlatio
215 oton-nitrogen correlations measured with the heteronuclear single quantum coherence (HSQC) experiment
217 s-[Pt(15NH3)2Cl2]1, are studied using 1H-15N heteronuclear single quantum coherence (HSQC) NMR and in
219 ects (KIEs) by (1)H-detected 2D [(13)C,(1)H]-heteronuclear single quantum coherence (HSQC) NMR spectr
220 erial completely and gave high-resolution 2D heteronuclear single quantum coherence (HSQC) NMR spectr
221 Results of NMR studies including 1H{15N} heteronuclear single quantum coherence (HSQC) show that
226 ive K296R kinase domain, and performed (15)N-heteronuclear single quantum coherence (HSQC) titrations
227 ar- and far-UV CD, and 1D and 2D ((1)H-(15)N heteronuclear single quantum coherence (HSQC)) NMR.
228 at straw, respectively, and characterized by heteronuclear single quantum coherence (HSQC), nuclear m
237 n agonist-bound conformation, as measured by heteronuclear single quantum coherence NMR, and lead to
239 ensional (1)H and two-dimensional (1)H/(13)C heteronuclear single quantum coherence nuclear magnetic
241 al shift perturbation analysis by (1)H-(15)N heteronuclear single quantum coherence spectra reveals d
242 nd hydrogen-deuterium exchange (using 1H-15N heteronuclear single quantum coherence spectra) reveal t
245 l (2D) NMR spectra, namely, (13)C-(1)H HSQC (heteronuclear single quantum coherence spectroscopy), (1
247 nation of heteronuclear NMR methods, such as heteronuclear single quantum coherence, HNCA, and HNCO,
248 lations (correlation spectroscopy, COSY, and heteronuclear single quantum coherence, HSQC) nuclear ma
249 substituents and can be readily assigned by heteronuclear single quantum coherence-nuclear magnetic
250 intermediate was undetectable in a series of heteronuclear single quantum coherences, revealing the d
252 correlation spectroscopy (COSY), (1)H-(31)P heteronuclear single quantum correlation (HSQC) and (1)H
253 or organophosphorus compounds via (31)P-(1)H heteronuclear single quantum correlation (HSQC) and prov
254 r Overhauser effect spectroscopy (NOESY) and heteronuclear single quantum correlation (HSQC) NMR spec
255 To address this issue, we recorded 1H-15N heteronuclear single quantum correlation (HSQC) spectra
257 adening of certain cross-peaks in the 15N-1H heteronuclear single quantum correlation (HSQC) spectrum
258 nuclear Overhauser enhancement spectroscopy heteronuclear single quantum correlation (NOESY-HSQC) NM
261 hat the protein fold was not disturbed using heteronuclear single quantum correlation NMR spectra.
262 ding monitored both by changes in (1)H-(15)N heteronuclear single quantum correlation spectra and by
263 and from natural abundance (13)C NMR, where heteronuclear single quantum correlation spectra reveal
264 in Escherichia coli and has a well dispersed heteronuclear single quantum correlation spectrum and a
266 ks for residues G13 to H19 in the (1)H-(15)N heteronuclear single quantum correlation spectrum sugges
267 oduced dispersed cross-peaks in a (1)H-(15)N heteronuclear single quantum correlation spectrum that e
269 il) can be reached with the (1)H-(13)C HSQC (Heteronuclear Single Quantum Correlation) experiment, th
271 a time, together with structural analysis by heteronuclear single quantum correlation-NMR spectroscop
272 cluster were fully elucidated by (13)C-(1)H heteronuclear single-quantum coherence (HSQC) in conjunc
274 r dichroism (CD) spectroscopy and (1)H-(15)N heteronuclear single-quantum coherence (HSQC) nuclear ma
276 ding, the kinetics of trypsin digestion, and heteronuclear single-quantum coherence nuclear magnetic
277 evidenced by multiple two-dimensional (15)N heteronuclear single-quantum coherence peaks for certain
278 F structure using nuclear magnetic resonance heteronuclear single-quantum coherence spectra of these
281 er dereplication, a differential analysis of heteronuclear single-quantum correlation (HSQC) spectra
283 ion spectroscopy (TOCSY) experiments, and 2D heteronuclear single-quantum correlation spectroscopy (H
284 n order of magnitude, compared to typical 2D heteronuclear single-quantum correlation-resolved diffus
289 st-free agents via SABRE with hyperpolarized heteronuclear spins, and thus is promising for biomedica
290 his approach into two- and three-dimensional heteronuclear SSNMR experiments to examine the MSP1D1 re
292 samples and between 1H and 31P-{1H} spectra (heteronuclear STOCSY) to recover latent metabolic inform
296 ombined with LC-MS, three-dimensional 19F-1H heteronuclear TOCSY filtered experiments based on this a
298 5)N chemical shift degeneracy we developed a heteronuclear zero-quantum (and double-quantum) coherenc
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