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   1 proton CSAs in fully protonated solids under magic angle spinning.                                   
     2 asing of individual spinning sidebands under magic angle spinning.                                   
     3  (13)C-(1)H residual dipolar couplings under magic-angle spinning.                                   
     4 he use of highly deuterated samples and fast magic-angle spinning.                                   
     5 observed by 13C solid-state NMR even without magic-angle spinning.                                   
     6 cho double-resonance (REDOR) technique under magic-angle spinning.                                   
     7 s virus (MeV) nucleocapsids under ultra-fast magic-angle spinning.                                   
     8 r burn trauma; and ex vivo, high-resolution, magic angle spinning (1)H NMR on intact excised mouse mu
  
  
  
    12 to the hydrophobic milieu, we carried out 2D magic-angle spinning (13)C NMR experiments on the water-
    13 ymer analysis was conducted using melt-state magic-angle spinning (13)C NMR spectroscopy of both line
  
    15  diffraction, solid-state cross-polarization/magic-angle spinning (13)C NMR, and Bloch-decay (13)C NM
    16 l (2D) and three-dimensional high-resolution magic-angle-spinning (13)C solid-state nuclear magnetic 
    17 SpSEEKFLRRIGRFG) are studied using deuterium magic angle spinning ((2)H MAS) line shape and spin-latt
  
  
  
    21 gin unit, were investigated with solid-state magic angle spinning (51)V NMR, FT-IR, in situ Raman, in
    22 lysis of the (77)Se{(1)H} cross-polarization magic angle spinning and (77)Se spin-echo solid-state NM
  
    24 gh-quality membrane protein samples for both magic-angle spinning and oriented-sample solid-state NMR
  
    26  ratio for solid-state NMR experiments under magic-angle spinning and static conditions, respectively
    27  rho) measurements, direct polarization with magic-angle spinning, and static CP of the hydrated and 
  
  
  
    31 We have adapted it to broad spectra and fast magic-angle spinning by accounting for long pulses (comp
    32 ange materials for data storage, even 22-kHz magic-angle spinning cannot resolve the center- and side
  
  
    35 atic liquid crystalline alignment, and under magic angle spinning conditions where alignment relative
    36  R1rho rates, which were measured under fast magic angle spinning conditions, vary by an order of mag
  
  
  
    40  experiment in liquids, is robust under fast magic-angle-spinning conditions and in the presence of d
  
  
  
    44 e line (2)H NMR and (13)C cross-polarization magic-angle spinning (CP-MAS) NMR spectra of Ala-PLB and
  
  
    47  various methods, such as cross-polarization magic angle spinning (CPMAS) (13)C NMR and single crysta
    48 ontact times were used in cross-polarization magic angle spinning (CPMAS) NMR, CP rotational-echo dou
    49 ta yielded orientational restraints, whereas magic-angle spinning data yielded interhelical distance 
  
    51 luded quantitative (13)C direct polarization/magic angle spinning (DP/MAS) and DP/MAS with recoupled 
    52 amically hyperpolarized (1)H to (13)C during magic-angle spinning dynamic nuclear polarization (DNP) 
  
    54 ing sPREs in practically the entire range of magic angle spinning frequencies used for biomolecular s
    55  application of (1)H-detected experiments at magic-angle spinning frequencies of >50 kHz enables the 
    56     The impact of the sample temperature and magic angle spinning frequency on epsilon is investigate
    57 ments (17.6, 20.0, and 23.5 T) and ultrafast magic angle spinning (>60 kHz), high-quality spectra wer
  
    59 changes during storage, (1)H high resolution-magic angle spinning (HR-MAS) NMR spectroscopy of apple 
  
  
  
  
  
    65  of C. elegans based on (1)H high-resolution magic-angle spinning (HR-MAS) nuclear magnetic resonance
    66 t tissue samples by means of high-resolution magic-angle-spinning (HR-MAS) NMR spectroscopy and we pr
    67  and metabolite analysis, by high-resolution magic angle spinning (HRMAS) (1)H NMR spectroscopy, in B
    68 nd subsequent application of high-resolution magic angle spinning (HRMAS) (1)H nuclear magnetic reson
    69 r metabolism was analyzed by high-resolution magic angle spinning (HRMAS) nuclear magnetic resonance 
    70 his paper describes a proton high resolution magic angle spinning (HRMAS) nuclear magnetic resonance 
  
  
    73 al, immunohistochemistry and high resolution magic angle spinning magnetic resonance spectroscopy (MR
  
  
    76 ptophan's interfacial preference by using 1H magic angle spinning (MAS) chemical shift measurements, 
    77 or all three compounds under both static and magic angle spinning (MAS) conditions at 21.1 T, allowin
    78 designed 3D (2)H-(13)C-(13)C solid-state NMR magic angle spinning (MAS) experiment is presented and d
    79 ancements of up to 23 have been obtained for magic angle spinning (MAS) experiments at 5 T and 85-90 
    80 H-(113)Cd and (1)H-(77)Se cross-polarization magic angle spinning (MAS) experiments, which demonstrat
  
    82 dard addition of water is combined with (1)H magic angle spinning (MAS) NMR detection, absolute quant
  
    84     We introduce a family of two-dimensional magic angle spinning (MAS) NMR experiments for structura
    85 st demonstration of natural-abundance (43)Ca magic angle spinning (MAS) NMR experiments on bone, usin
    86 e we report atomic-level characterization by magic angle spinning (MAS) NMR of the muscle isoform of 
  
    88 es in the 17O high-resolution triple-quantum magic angle spinning (MAS) NMR spectra were resolved and
  
    90 reviously we have demonstrated the use of 1H magic angle spinning (MAS) NMR spectroscopy for the topo
  
  
  
  
    95 otopic substitution (NDIS) techniques, (6)Li Magic Angle Spinning (MAS) NMR spectroscopy, and for the
  
  
  
    99 the fibril formation process in vitro, and a magic angle spinning (MAS) NMR study of the fibrils form
   100 pic labeling strategies and multidimensional magic angle spinning (MAS) NMR techniques at high magnet
  
  
  
  
  
   106 absorption fine structure (EXAFS) and (27)Al magic angle spinning (MAS) nuclear magnetic resonance (N
   107 ce-specific backbone resonance assignment of magic angle spinning (MAS) nuclear magnetic resonance (N
   108 cy driven dipolar recoupling (RFDR) and (1)H magic angle spinning (MAS) nuclear Overhauser effect spe
  
  
  
   112  of oriented sample (OS) solid-state NMR and magic angle spinning (MAS) solid-state NMR techniques to
  
   114 ctural forms and examined the specimens with magic angle spinning (MAS) solid-state nuclear magnetic 
   115 13)C(alpha) dipolar coupling, stationary and magic angle spinning (MAS) spectra with and without (15)
  
   117 vity on natural abundance samples using fast magic angle spinning (MAS), indirect detection of low-ga
  
  
   120  field of dynamic nuclear polarization under magic angle spinning (MAS-DNP) could be used to dramatic
   121  The 2D NMR spectra were acquired under fast magic-angle spinning (MAS) and dipolar-assisted rotation
   122 )C dynamic nuclear polarization at 5 T under magic-angle spinning (MAS) at 82 K using a mixture of mo
  
  
   125 peptides or proteins by measuring RDCs using magic-angle spinning (MAS) in combination with dipolar r
   126 rphs by a combination of stationary and fast magic-angle spinning (MAS) methods at high magnetic fiel
   127 blies in the escape from CypA dependence, by magic-angle spinning (MAS) NMR and molecular dynamics (M
   128  powder XRD, (1)H double-quantum solid-state magic-angle spinning (MAS) NMR and small-angle neutron s
  
  
  
   132 n structure determination by proton-detected magic-angle spinning (MAS) NMR has focused on highly deu
  
   134 ic reaction centers (RCs) as modification of magic-angle spinning (MAS) NMR signal intensity under il
  
  
  
  
   139 y depends on their dynamics, and solid-state magic-angle spinning (MAS) nuclear magnetic resonance (N
  
   141 ere we report sample preparation and initial magic-angle spinning (MAS) solid-state NMR (SSNMR) of CY
  
  
  
   145 ation of 1H, 13C, and 15N chemical shifts by magic-angle spinning (MAS) solid-state NMR with first-pr
   146 I3-SH3 in amyloid fibril form as revealed by magic-angle spinning (MAS) solid-state nuclear magnetic 
  
  
  
   150 ion of 13C and 15N NMR chemical shifts under magic-angle spinning (MAS), effects of local mobility on
  
  
  
   154 S31N mutant of M2(18-60) determined using 3D magic-angle-spinning (MAS) NMR spectra acquired with a (
  
  
  
  
   159 ng (R(3)) combined with the multiple-quantum magic-angle spinning (MQMAS) in a three-dimensional (3D)
   160 , based on a series of temperature-dependent magic-angle spinning multinuclear nuclear-magnetic-reson
  
   162 ound to end-binding protein EB1 and free, by magic angle spinning NMR and molecular dynamics simulati
  
   164 th solid-state wide-line and high resolution magic angle spinning NMR as well as with fluorescence co
  
  
  
   168 version by solid state (13)C cross-polarized magic angle spinning NMR reveals that solid heptacene ha
  
   170 rovided by analysis of 2D rotor-synchronized magic angle spinning NMR spectra of doubly 13C carbonyl 
  
  
  
   174  NMR crystallography approach based on (51)V magic angle spinning NMR spectroscopy and Density Functi
   175 e to detailed structural characterization by magic angle spinning NMR spectroscopy and that solid-sta
  
   177 nts of vanadium have been addressed by (51)V magic angle spinning NMR spectroscopy of six-coordinated
   178 nge interhelical distance measurements using magic angle spinning NMR spectroscopy provide high-resol
  
  
  
   182 ransgenic mouse model using a combination of magic angle spinning NMR spectroscopy, in silico predict
  
  
  
  
  
  
  
  
  
   192 ol) in monounsaturated model membranes using magic angle spinning NMR to measure these interactions t
  
   194 dividual bilayer lipids was studied by (31)P magic angle spinning NMR, and toxin-induced changes in b
   195 eled agonist CP-55,940-d(6) measured by (2)H magic angle spinning NMR, as well as by activation of G 
   196 an array of approaches (limited proteolysis, magic angle spinning NMR, Fourier transform infrared spe
   197 ng this protocol, proteoliposome samples for magic-angle spinning NMR and uniformly aligned samples (
  
  
   200 mensional (2D) solid-state (29)Si and (27)Al magic-angle spinning NMR methodologies, including T(1)-r
  
  
   203  NMR experiments that enhance sensitivity in magic-angle spinning NMR spectra of cryo-trapped photocy
  
  
  
   207  This approach combining oriented-sample and magic-angle spinning NMR spectroscopy in native-like lip
   208 lved spectrum, obtained from high-resolution magic-angle spinning NMR spectroscopy of liver tissues, 
  
  
   211  study provides, to our knowledge, the first magic-angle spinning NMR structure of an intact filament
   212 es of CP-55,940 and POPC were measured by 1H magic-angle spinning NMR with pulsed magnetic field grad
  
   214 e been observed by performing double-quantum magic-angle-spinning NMR at low temperature in the prese
  
   216  shift anisotropy (CSA) tensors, recorded in magic-angle-spinning NMR experiments, provide direct res
  
  
   219  microscopy and circular dichroism and (11)B magic-angle-spinning NMR spectroscopy, is stable in wate
  
  
  
  
  
   225 bility of dynamic nuclear polarization (DNP) magic-angle-spinning NMR techniques, along with a judici
   226 y induced dynamic nuclear polarization) MAS (magic angle spinning) NMR demonstrates that indeed the p
   227  at low temperature and high viscosity) MAS (magic angle spinning) NMR that both populations are pres
   228 tion of solid-state (13)C-cross-polarization magic angle spinning nuclear magnetic resonance ((13)C-C
   229 spectroscopy (XAS), (13)C Cross polarization-magic angle spinning nuclear magnetic resonance (CP-MAS 
  
   231 mography, complemented with (27)Al and (31)P magic angle spinning nuclear magnetic resonance (MAS NMR
   232 ration of multilamellar lipid vesicles using magic angle spinning nuclear magnetic resonance has been
   233 9 kDa paramagnetic enzyme, using solid-state magic angle spinning nuclear magnetic resonance methods.
   234 rphism based on sideband analyses of the 31P magic angle spinning nuclear magnetic resonance spectra.
   235 ders of magnitude in length scale--including magic angle spinning nuclear magnetic resonance spectros
   236 ructure of Nafion 211 using calibrated (19)F magic angle spinning nuclear magnetic resonance spectros
   237 e matrix were investigated using solid-state magic angle spinning nuclear magnetic resonance spectros
  
   239 ing a variety of techniques, including (31)P magic angle spinning nuclear magnetic resonance, and are
  
  
   242 we utilized state-of-the-art high-resolution magic-angle spinning nuclear magnetic resonance (HRMAS N
   243 )3 NASICON series has been analyzed by (31)P magic-angle spinning nuclear magnetic resonance (MAS NMR
   244 P dipolar heteronuclear correlation (HETCOR) magic-angle spinning nuclear magnetic resonance (NMR) is
  
   246 ion of ultrahigh magnetic field, solid-state magic-angle spinning nuclear magnetic resonance spectros
   247 esicles were studied using (31)P solid-state magic-angle-spinning nuclear magnetic resonance spectros
  
   249 lies that are stable and are not affected by magic angle spinning of the samples at frequencies betwe
  
   251 f the protein in combination with high-speed magic angle spinning produces (1)H resonances averaging 
   252 tatectomy were analyzed with high-resolution magic angle spinning proton magnetic resonance spectrosc
   253 tate NMR measurements at very fast (100 kHz) magic-angle spinning rates and at high (23.5 T) magnetic
   254 inescent scaffolds, (13)C cross-polarization magic angle spinning solid-state (CP-MAS) NMR spectrosco
  
  
  
  
   259 shift data and interhelical cross peaks from magic angle spinning solid-state NMR of a liposomal prep
   260 is, FT-IR, UV-vis diffuse reflectance, (31)P magic angle spinning solid-state NMR spectroscopy, and p
  
  
  
   264 t with dynamic nuclear polarization enhanced magic angle spinning solid-state NMR to study this chall
  
  
  
  
   269 guided by structure restraints obtained from magic-angle spinning solid-state NMR experimental data. 
   270 or dual data acquisition of multidimensional magic-angle spinning solid-state NMR experiments is pres
   271 eled octasaccharide heparin analogue enabled magic-angle spinning solid-state NMR of the GAG bound to
   272 ignments are presented for resonances in the magic-angle spinning solid-state NMR spectra of the majo
   273 ntroduce an iterative approach that combines magic-angle spinning solid-state NMR spectroscopy and at
  
  
   276 mical shift assignments of large proteins by magic-angle spinning solid-state NMR, using the 21-kDa d
  
   278 rotein structure determination methods using magic-angle spinning solid-state nuclear magnetic resona
   279 itates rapid acquisition of multidimensional magic-angle spinning solid-state nuclear magnetic resona
   280 n function (PDF) analysis and ex situ (23)Na magic-angle spinning solid-state nuclear magnetic resona
  
  
  
  
  
  
  
   288  stationary amides and "solution-like" (13)C magic angle spinning spectra at 75 degrees C, at which t
  
   290 e-bound RTD-1 exhibits narrow line widths in magic-angle spinning spectra, but the sideband intensiti
  
  
   293 e-dimensional CPMAS (cross-polarization with magic angle spinning) techniques, including spectral edi
   294 we demonstrate through (13)C high-resolution magic-angle-spinning that (13)C acetate from fermentatio
   295  with one being performed at high-resolution magic-angle spinning to obtain pure J-couplings without 
   296 bservable with single pulse excitation using magic angle spinning until the sample temperature reache
   297 al shift anisotropy (CSA) is recoupled under magic-angle spinning using the SUPER technique to yield 
   298 onsidered essentially as a solid-state, slow-magic-angle-spinning version of the distortionless enhan
   299 sional heteronuclear NMR in conjunction with magic-angle spinning, we have identified chemical bondin
   300  (13)C chemical shift spectra obtained under magic-angle spinning were used evaluate the dehydration-
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