ライフサイエンスコーパス: saponification

1 d derivative 19 with diethyl L-glutamate and saponification.

2 coupled with diethyl l-glutamate followed by saponification.

3 coupled with diethyl L-glutamate followed by saponification.

4 coupled with diethyl-l-glutamate followed by saponification.

5 up compatibility of beta-hydroxy phosphonate saponification.

6 resistance of the product of the reaction to saponification.

7 ma was analyzed in a similar way but without saponification.

8 target analogues 10 were readily prepared by saponification.

9 4 which was converted to 3a by reduction and saponification.

10 ied base concentration and the total time of saponification across a wide range and again used HPLC t

11 ones, coupling with diethyl-L-glutamate, and saponification afforded 2-5.

12 ing 8 with L-glutamic acid diethyl ester and saponification afforded 2.

13 oisomer with diethyl-l-glutamate followed by saponification afforded 4 and 5.

14 equent coupling with diethyl l-glutamate and saponification afforded target compounds 3a-d.

15 diethyl ester, followed by hydrogenation and saponification, afforded 1-3.

16 However, saponification also hydrolyses esterified carotenoids an

17 After saponification and base-induced cleavage of the N-phenyl

18 Ester saponification and decarboxylation with KOH in ethylene

19 Recovery of the saponification and extraction was demonstrated via analy

20 results of four soybeans using the described saponification and HPLC analytical method was validated

21 The acid, peroxide, saponification and iodine values and unsaponifiable matt

22 Ester saponification and protecting group manipulation provide

23 tion periods of 20 min, followed by alkaline saponification and purification of the extracts.

24 hlorophyll removal mechanism is not based on saponification, apolar adsorption or anion exchange, but

25 -6-(bromomethyl)-pteridine followed by ester saponification at room temperature to afford the respect

26 recovered with strong base after 6 hours of saponification at room temperature.

27 ves the corresponding amino ester that, upon saponification, can be protected with the fluorenylmethy

28 with trimethylsulfoxonium ylide, followed by saponification, completed a five-step synthesis of 1 in

29 tion of the beta-indole-alpha-oximinoesters, saponification, condensation with symmetrical diamines,

30 To assess the effects of saponification conditions on carotenoid recovery from qu

31 arachidonoyl)-phosphatidylethanolamine under saponification conditions, and the amount produced incre

32 very of epsilon-carotene was not affected by saponification conditions.

33 Astaxanthin was sensitive to saponification conditions; recovery was poor with strong

34 standards were added as surrogates prior to saponification, correcting for extraction inefficiencies

35 pimerization of the ester center followed by saponification/crystallization affords the desired hydro

36 Saponification ensured complete extraction of retinol an

37 erial from the Eskimo mummy was subjected to saponification, extraction, and digitonin precipitation.

38 Culture, harvesting, saponification, extraction, derivatization, and chromato

39 A saponification/extraction procedure and high performance

40 Their deprotection by ester saponification followed by hydrogenolysis yielded the fr

41 terol was isolated from whole yeast cells by saponification, followed by extraction of nonsaponifiabl

42 Saponification gave 21,23-dithiaporphyrin dicarboxylate

43 diluted in hexane without derivatisation or saponification, greatly reducing sample preparation time

44 scalemic diesters 4 with t-BuLi, followed by saponification in the presence of air, gave 2,2'-di-tert

45 y acidity, peroxide, iodine, refractive, and saponification indexes, beyond moisture, lipid and free

46 rted in five steps (reduction of the ketone, saponification, iodolactonization, ozonolysis, and intra

47 Alkaline saponification is often used to remove interfering chlor

48 o avoid carotenoid artifact formation during saponification, Larsen and Christensen (2005) developed

49 They hypothesised a saponification mechanism based on their Liquid Chromatog

50 In the latter setting, saponification must precede the diol cleavage step which

51 The ranges of saponification number (199.2-202.1), iodine value (104.8

52 l and chemical parameters (melting point and saponification number), and the fraction of hydrocarbons

53 Saponification of (-)-heptemerone afforded (-)-guanacast

54 Saponification of (14)C-labeled 18:3-16:3-MGDG revealed

55 Saponification of 15 and reaction with 50% aqueous NH(2)

56 Saponification of arnottin I and hypervalent iodide medi

57 ine F, and fragments 88 and 89 obtained upon saponification of batzelladine F, demonstrated that the

58 AEA (>1 nmol/g) was produced during saponification of brain phospholipid extracts.

59 ters are accessible by the selective partial saponification of dimethyl or diethyl alkyl phosphonates

60 Following saponification of extracted lipids, fatty acid phenacyl

61 By partial saponification of isolated foreskin epidermal CEs follow

62 nfrared spectroscopy (FTIR) follow-up of the saponification of oil by lead compounds.

63 Also, saponification of plasma samples was determined to cause

64 e percentage of KOH (60% and 80% w/v) in the saponification of samples for the determination of alpha

65 On saponification of the 3- and 4-substituted benzoates, th

66 eria in an extraction vessel resulted in the saponification of the bacterial lipids and derivatizatio

67 ing opening with cesium benzoate followed by saponification of the benzoate to afford (+)-pancratista

68 al of the borane under acidic conditions and saponification of the ester.

69 anopyrrolo[2,3-d]pyrimidine (28) followed by saponification of the ethyl esters, for the classical an

70 Saponification of the lipid released a water-soluble hea

71 In addition, saponification of the primary Alder-ene product derived

72 The method consists in the direct saponification of the sample and purification of oxyster

73 Saponification of the separated bismenthyl carbonates ga

74 the primary alcohol group in 50 followed by saponification of the two remaining ester groups gave 3.

75 Saponification of these C60 multiple adducts gives the c

76 AEA generated during saponification of tissue phospholipids appears to arise

77 the cyclopentenones (e.g., demethylation and saponification) of the CNTs lead to demethylated or hydr

78 e solubilized by proteolytic digestion after saponification, of which involucrin was the most abundan

79 ted after sample preparation, extraction and saponification (only when strictly necessary).

80 quisite triesters were prepared by selective saponification or by the prior incorporation of one benz

81 acid and amine derivatives were obtained by saponification or HCl acidolysis of o-boronato-phosphoni

82 aces analysis showed that the most efficient saponification procedure was obtained using a 60% (w/v)

83 tina, and to assess the effects of different saponification procedures on the recovery of quail retin

84 The simplified one-step extraction without saponification significantly increased the recovery of t

85 total time of extraction for 300s regarding saponification step when compared to 3600s from the trad

86 ally, it was proposed for the removal of the saponification step, which simplifies the extraction pro

87 actosyl halides 12a,b and 26 afforded, after saponification, the desired aryl glycosides 7a,b.

88 rent preparative parameters, such as time of saponification, the type of organic solvents for fat ext

89 ical dipyrrylmethane 19, and following ester saponification, this was condensed with a dipyrrylmethan

90 of simultaneously extracting sterols during saponification thus significantly reducing extraction ti

91 he benzyl halide for alkylation, followed by saponification to afford 7.

92 goes a kinetically controlled epimerization/ saponification to afford the pure trans-pyrrolidine carb

93 l ester of ciprofloxacin (11) to give, after saponification to remove all of the esters, the desired

94 iabetic rats, before and after conversion by saponification to the corresponding DKP insulin enantiom

95 reated human foreskin CEs with methanol/KOH (saponification) to hydrolyze off much of the lipids.

96 oupled with diethyl-L-glutamate, followed by saponification, to give the target compounds 2-8.

97 ne in the HPLC autosampler and the effect of saponification upon lycopene isomerization.

98 g of oil), acid value (2.36mg KOH/g of oil), saponification value (183.8mg KOH/g of oil), peroxide va

99 Increases in the density, viscosity, saponification value and oxidation of the oil were detec

100 ere as follows: melting point, 45 degrees C; saponification value, 202.3 mg KOH/g oil; refractive ind

101 s (4.9-68.9), iodine values (93.3-160.4) and saponification values (65.9-117.9).

102 The seed oil had higher acid and saponification values and low iodine value.

103 atty acids extracted from cell pellets after saponification were analyzed by gas chromatography/mass

104 , quantification and the critical aspects of saponification were investigated and optimised.

105 Adipose tissue necrosis and saponification were present in cytokine-injected ob/ob b

106 ts were dissolved in chloroform with help of saponification with 1M solution of sodium hydroxide in u

107 Ester saponification with aqueous NaOH followed by a two-step

108 Extraction is performed without saponification, with the aid of protease to remove vitam

109 Saponification yields 2-alkylindanones, providing, in ef